Medicinal plants are the major source of therapeutics and pharmaceutical industries. Phytochemicals present in plants are used in many ways for betterments of mankind’s. The study of Soymida febrifuga with focusing its leves is associated to the medicinal properties of plant. Many research workers reported ethno medicinal aspects of plants. The current works is find phytochemical properties and therapeutics aspects of Soymida febrifuga with the help of modern analysis techniques like FTIR and GC MS analysis with standard methodology. The significant result was recorded as per GC MS data and further analyzed with analyzed results with data of National Institute of Standards and Technology (NIST) and on Dr. Duke’s Phytochemical and tthno botanical Databases.